منابع مشابه
Solid–Solid Synthesis, Crystal Structure and Thermal Decomposition of Copper(II) Complex of 2-Picolinic Acid
The copper(II) complex [Cu(pic)2]·2H2O was synthesized with 2-picolinic acid (Hpic) and copper acetate as reactants by room temperature solid-solid reaction. The composition and structure of the complex was characterized by elemental analyses, single crystal X-ray diffraction, X-ray powder diffraction, FT-IR spectroscopy and thermogravimetry-differential scanning calor...
متن کاملsolid–solid synthesis, crystal structure and thermal decomposition of copper(ii) complex of 2-picolinic acid
the copper(ii) complex [cu(pic)2]·2h2o was synthesized with 2-picolinic acid (hpic) and copper acetate as reactants by room temperature solid-solid reaction. the composition and structure of the complex was characterized by elemental analyses, single crystal x-ray diffraction, x-ray powder diffraction, ft-ir spectroscopy and thermogravimetry-differential scanning calorimetry. the crystal struct...
متن کاملSynthesis of Single-Crystalline Octahedral Co3O4 with Solid-State Thermal Decomposition
In this paper, single crystalline octahedral Co3O4 with dimensions about 100–500 nm and smooth surface has been prepared by solid-state thermal decomposition of cobalt(II) Schiff base complex Co((3,4-MeO-ba)2 en)Cl2 as new precursor at 450ºC under air atmosphere for 3.5 h. Surface morphology of the products were characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray powder ...
متن کاملSynthesis and characterization of nanowires Hausmannite (Mn3O4) by solid-state thermal decomposition
In this study, we synthesis one-dimensional (1D) manganese(III) Schiff base coordination polymer [Mn(Brsalophen)(μ1,3-N3)]n by reaction of MnCl2·6H2O and tetradentate Schiff base ligand Brsalophen at the presence of NaN3 in methanol and characterized by elemental analyses (CHN) and FT-IR spectroscopy. It was used as a new precurs...
متن کاملSynthesis and characterization of nanowires Hausmannite (Mn3O4) by solid-state thermal decomposition
In this study, we synthesis one-dimensional (1D) manganese(III) Schiff base coordination polymer [Mn(Brsalophen)(μ1,3-N3)]n by reaction of MnCl2·6H2O and tetradentate Schiff base ligand Brsalophen at the presence of NaN3 in methanol and characterized by elemental analyses (CHN) and FT-IR spectroscopy. It was used as a new precurs...
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ژورنال
عنوان ژورنال: Chemical engineering
سال: 1961
ISSN: 0375-9253
DOI: 10.1252/kakoronbunshu1953.25.265